Organic Chemistry I Laboratory
(Summer I 2025)
CHEM 0203 (T 12:00-3:00, R 12:00-3:00)
Lab Schedule

Date

Activity

May 19

Monday
Check In

May 20

Tuesday
Lewis Structures handout will be distributed in lab.
Due: Hand in Lewis Structures worksheet before leaving lab.

May 22

Thursday
Recrystallization of Benzoic Acid is available here.
Remember to save your benzoic acid so that you can determine its melting point in a future lab meeting.

May 27

Tuesday
Isolating Natural Products (Caffeine): Liquid-liquid extraction is available here.
Remember to save your crude caffeine so that you can purify it next lab.

May 29

Thursday
Determine the melting point of your benzoic acid and sublime your caffeine

June 3

Tuesday
Co-Distillation: The isolation of eugenol from cloves is available here.
Remember to save your clove oil for analysis next lab.
Due: Hand in your report for the Recrystallization of Benzoic Acid activity.
Due: Hand in your report for the Isolating Natural Products (Caffeine): Liquid-liquid extraction activity.

June 5

Thursday
An Introduction to the Gas Chromatograph: Collecting a chromatogram of clove oil is available here

June 10

Tuesday
Regioselectivity: Electrophilic addition and bromohydrin formation is available here. We will synthesize the bromohydrin this lab and perform chemical tests on it next lab.
Additional information about the lab is available here. The page contains videos and a flow chart that will help you understand the procedures followed during the experiment. The videos also show how the apparatuses used in the activity are set up.
Due: Hand in the report for An Introduction to the Gas Chromatograph: Collecting a chromatogram of clove oil

June 12

Thursday
Finish Regioselectivity: Electrophilic addition and bromohydrin formation
AND start Stereospecificity: Electrophilic addition and bromohydrin formation, which is available here.
Additional information about the lab is available here. The page contains videos and a flow chart that will help you understand the procedures followed during the experiment. The videos also show how the apparatuses used in the activity are set up.

June 17

Tuesday
Finish Stereospecificity: Electrophilic addition and bromohydrin formation
Due: Regioselectivity: Electrophilic addition and bromohydrin formation report.

June 19

Thursday
Nucleophilic Substitution: Nucleophilicity and mechanistic effects can be downloaded from here.
Due: Stereospecificity: Electrophilic addition and bromohydrin formation report.

June 24

Tuesday
Alkene Formation: Dehydrohalogenation of 1- and 2-bromobutane and dehydration of 1- and 2-butanol is available here.
Here is a web page with additional information about the dehydration and dehydrohalogenation activity. The page contains videos that will help you understand the procedures followed during the experiment and how the apparatuses used in the activity are set up.

June 26

Thursday
Check Out
Due: Nucleophilic Substitution: Nucleophilicity and mechanistic effects report.
Due: Alkene Formation: Dehydrohalogenation of 1- and 2-bromobutane and dehydration of 1- and 2-butanol report.

PLEASE NOTE: Preparing a pre-lab (writing down the goal of the activity in the reaction section, looking up the properties and hazards associated with the chemicals being used and writing them down in the materials section, and writing down a plan/procedure that will be followed in lab) in your notebook before coming to lab is an important process that will help you complete the laboratory activities succesfully; thus, write-ups may be checked at the beginning of the laboratory period.

The faculty teaching this course reserve the right to unilaterally alter the schedule as needed. Any changes to the schedule will be announced in class and recorded in this document.